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Year 2023, Volume: 11 Issue: 2, 204 - 215, 25.12.2023

Berdan Ulaş

https://doi.org/10.51354/mjen.1312700

Abstract

References

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Response surface methodology optimization of electrode modification parameters toward hydrazine electrooxidation on Pd/MWCNT/GCE

Year 2023, Volume: 11 Issue: 2, 204 - 215, 25.12.2023

Berdan Ulaş

https://doi.org/10.51354/mjen.1312700

Abstract

In this study, MWCNT supported Pd (Pd/MWCNT) was synthesized by NaBH4 reduction method as catalyst for hydrazine electrooxidation reaction (HEOR). Characterization methods namely inductively coupled plasma mass spectrometry (ICP-MS), elemental mapping, and scanning electron microscopy with energy dispersive X-ray (SEM-EDX) were used to analyze the surface morphology and metal composition of the catalysts. The Pd/MWCNT catalyst's average particle size is estimated to be 6.35 nm based on SEM images. Glassy carbon electrode (GCE) modification parameters namely the amount of catalyst ink transferred to the GCE surface (Vs), ultrasonication time of the catalyst ink (tu), and the drying time of the Pd/MWCNT/GCE (td) were optimized by using response surface methodology as 4.92 μL, 1 min and 19.52 min, respectively. Experimental specific activity value for HEOR was obtained as 7.13 mA cm-2 with 2.59% deviation under optimum conditions. Optimization of electrode preparation conditions is an inexpensive and facile method that could be used to improve the performance of anode catalysts for fuel cells.

Keywords

response surface methodology hydrazine electrocatalyst

References

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  • [21]. Li, J., Dong, C., Guo, M., Gao, W., Kang, L., Lei, F., Hao, P., Xie, J., Tang, B. "Cerium-Induced Lattice Disordering in Co-Based Nanocatalysts Promoting the Hydrazine Electro-Oxidation Behavior", Chemical Communications, 58, (2022), 6845-6848; Feng, G., An, L., Li, B., Zuo, Y., Song, J., Ning, F., Jiang, N., Cheng, X., Zhang, Y., Xia, D. "Atomically Ordered Non-Precious Co3ta Intermetallic Nanoparticles as High-Performance Catalysts for Hydrazine Electrooxidation", Nature Communications, 10, (2019), 4514; Firdous, N., Janjua, N. K. "Coptx/Γ-Al2o3 Bimetallic Nanoalloys as Promising Catalysts for Hydrazine Electrooxidation", Heliyon, 5, (2019), e01380.
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There are 29 citations in total.

Details

Primary Language English
Subjects Electrochemical Technologies
Journal Section Research Article
Authors

Berdan Ulaş 0000-0003-0650-0316

Publication Date December 25, 2023
Published in Issue Year 2023 Volume: 11 Issue: 2

Cite

APA Ulaş, B. (2023). Response surface methodology optimization of electrode modification parameters toward hydrazine electrooxidation on Pd/MWCNT/GCE. MANAS Journal of Engineering, 11(2), 204-215. https://doi.org/10.51354/mjen.1312700
AMA Ulaş B. Response surface methodology optimization of electrode modification parameters toward hydrazine electrooxidation on Pd/MWCNT/GCE. MJEN. December 2023;11(2):204-215. doi:10.51354/mjen.1312700
Chicago Ulaş, Berdan. “Response Surface Methodology Optimization of Electrode Modification Parameters Toward Hydrazine Electrooxidation on Pd/MWCNT/GCE”. MANAS Journal of Engineering 11, no. 2 (December 2023): 204-15. https://doi.org/10.51354/mjen.1312700.
EndNote Ulaş B (December 1, 2023) Response surface methodology optimization of electrode modification parameters toward hydrazine electrooxidation on Pd/MWCNT/GCE. MANAS Journal of Engineering 11 2 204–215.
IEEE B. Ulaş, “Response surface methodology optimization of electrode modification parameters toward hydrazine electrooxidation on Pd/MWCNT/GCE”, MJEN, vol. 11, no. 2, pp. 204–215, 2023, doi: 10.51354/mjen.1312700.
ISNAD Ulaş, Berdan. “Response Surface Methodology Optimization of Electrode Modification Parameters Toward Hydrazine Electrooxidation on Pd/MWCNT/GCE”. MANAS Journal of Engineering 11/2 (December 2023), 204-215. https://doi.org/10.51354/mjen.1312700.
JAMA Ulaş B. Response surface methodology optimization of electrode modification parameters toward hydrazine electrooxidation on Pd/MWCNT/GCE. MJEN. 2023;11:204–215.
MLA Ulaş, Berdan. “Response Surface Methodology Optimization of Electrode Modification Parameters Toward Hydrazine Electrooxidation on Pd/MWCNT/GCE”. MANAS Journal of Engineering, vol. 11, no. 2, 2023, pp. 204-15, doi:10.51354/mjen.1312700.
Vancouver Ulaş B. Response surface methodology optimization of electrode modification parameters toward hydrazine electrooxidation on Pd/MWCNT/GCE. MJEN. 2023;11(2):204-15.
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